| Place of Origin: | China |
|---|---|
| Brand Name: | First |
| Certification: | COA |
| Model Number: | 28578-16-7 |
| Minimum Order Quantity: | 1KG |
| Price: | 50-100USD |
| Packaging Details: | 1kg/bag ;25kg/drum,25 kg/Carton |
| Delivery Time: | 5 to 10 days |
| Payment Terms: | L/C, D/A, D/P, T/T, Western Union, MoneyGram,BTC |
| Supply Ability: | 1000 Tons |
| Purity: | 99.0%min | Type: | Syntheses Material Intermediates |
|---|---|---|---|
| Appearance: | White Crystal | Cas No.: | 28578-16-7 |
| Mf: | C13H14O5 | Other Names: | 3-(1,3-benzodioxol-5-yl)-2-Methyl- |
| Einecs No.: | 234-232-0 | Product Name: | PMK Ethyl Glycidate |
| Density: | 1.302±0.06 G/cm3(Predicted) | Sample: | Availiable |
| High Light: | Pmk Chemical Powder,White Crystal Fertilizer In Laboratory Resarch,Pmk White Crystal Fertilizer |
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Synonyms:3-(1,3-benzodioxol-5-yl)-2-Methyl-;3,4-MDP-2-P intermediate;PMK ethyl glycidate;2-Oxiranecarboxylicacid, 3-(1,3-benzodioxol-5-yl)-2-Methyl-, ethyl ester;ethyl 3-(benzo[d][1,3]dioxol-5-yl)-2-methyloxirane-2-carboxylate;ethyl 3-(1,3-benzodioxol-5-yl)-2-methyloxirane-2-carboxylate;
| Product Name: | PMK ethyl glycidate |
| CAS: | 28578-16-7 |
| MF: | C13H14O5 |
| MW: | 250.25 |
| EINECS: | 234-232-0 |
| Mol File: | 28578-16-7.mol |
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| Boiling point | 327.8±42.0 °C(Predicted) |
| density | 1.302±0.06 g/cm3(Predicted) |
| solubility | DMF: 15 mg/ml; DMSO: 30 mg/ml; Ethanol: 10 mg/ml; PBS (pH 7.2): 1 mg/ml |
| Description | PMK ethyl glycidate is an analytical reference standard categorized as a precursor in the synthesis of phenethylamines and amphetamines. |
| Uses | Methyl pepper epoxy ethyl propionate can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development process and pharmaceutical chemical production process. PMK ethyl glycidate (NSC 195099) is a precursor of M-ALPHA-HMCA. |
| Synthesis | To a solution of piperonal (1, 3.00 g, 19.9 mmol) in CH2Cl2 (100 mL) was added (carbethoxyethylidene)triphenylphosphorane (2,14.5 g, 40.0 mmol), and the reaction mixture was stirred for 24 h at room temperature. The mixture was then concentrated at reduced pressure, and the residue was purified by flash column chromatography on silica gel (hexanes/EtOAc,10:1) to afford olefin 3 (4.45 g, 95%) as a colorless oil |
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